- Size Control of Nd-Fe-B Precursor Particles Prepared by Spray Drying and Its Effect on the Magnetic Properties of Nd-Fe-B Alloy Powders after Reduction-Diffusion
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Youn-Kyoung Baek, Young-Taek Seo, Jung-Goo Lee, Dong Su Kim, Dong Sik Bae, Chul-Jin Choi
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J Korean Powder Metall Inst. 2013;20(5):359-365.
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DOI: https://doi.org/10.4150/KPMI.2013.20.5.359
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- In this study, we fabricated Nd_2Fe_14B hard magnetic powders with various sizes via spray drying combined with reduction-diffusion process. Spray drying is widely used to produce nearly spherical particles that are relatively homogeneous. Thus, the precursor particles were prepared by spray drying using the aqueous solution containing Nd salts, Fe salts and boric acid with the target stoichiometric composition of Nd_2Fe_14B. The mean particle sizes of the spray-dried powders are in the range from one to seven micrometer, which are adjusted by controlling the concentrations of precursor solutions. After debinding the as-prepared precursor particles, ball milling was also conducted to control the particle sizes of Nd-Fe-B oxide powders. The resulting particles with different sizes were subjected to subsequent treatments including hydrogen reduction, Ca reduction and washing for CaO removal. The size effect of Nd-Fe-B oxide particles on the formation of Nd_2Fe_14B phase and magnetic properties was investigated.
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Citations
Citations to this article as recorded by  - Research trend in Fabrication of Metastable-phase Iron Nitrides for Hard Magnetic Applications
Kyung Min Kim, Jung-Goo Lee, Kyung Tae Kim, Youn-Kyoung Baek
Journal of Korean Powder Metallurgy Institute.2019; 26(2): 146. CrossRef - Synthesize of Nd2Fe14B Powders from 1-D Nd2Fe14B Wires using Electrospinning Process
Nu Si A Eom, Su Noh, Muhammad Aneeq Haq, Bum Sung Kim
Journal of Korean Powder Metallurgy Institute.2019; 26(6): 477. CrossRef
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