- Production of Fe Amorphous Powders by Gas-atomization Process and Subsequent Spark Plasma Sintering of Fe Amorphous-ductile Cu Composite Powders Produced by Ball-milling Process (I) - I. Gas Atomization and Production of Composite Powders -
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Ho-Jin Ryu, Jae-Hyun Lim, Ji-Soon Kim, Jin-Chun Kim, H.J. Kim
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J Korean Powder Metall Inst. 2009;16(5):316-325.
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DOI: https://doi.org/10.4150/KPMI.2009.16.5.316
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Abstract
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- Fe based (Fe_68.2C_5.9Si_3.5B_6.7P_9.6Cr_2.1Mo_2.0Al_2.0) amorphous powder, which is a composition of iron blast cast slag, were produced by a gas atomization process, and sequently mixed with ductile Cu powder by a mechanical ball milling process. The experiment results show that the as-prepared Fe amorphous powders less than 90 mum in size has a fully amorphous phase and its weight fraction was about 73.7%. The as-atomized amorphous Fe powders had a complete spherical shape with very clean surface. Differential scanning calorimetric results of the as-atomized Fe powders less than 90 mum showed that the glass transition, T_g, onset crystallization, T_x, and super-cooled liquid range DeltaT=T_x-T_g were 512, 548 and 36°C, respectively. Fe amorphous powders were mixed and deformed well with 10 wt.% Cu by using AGO-2 high energy ball mill under 500 rpm.
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