- Fabrication and Characterization of Porous Nickel Membrane for High Precision Gas Filter by In-situ Reduction/Sintering Process
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Nam-Hoon Kim, Han-Bok Song, Sung-Churl Choi, Yong-Ho Choa
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J Korean Powder Metall Inst. 2009;16(4):262-267.
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DOI: https://doi.org/10.4150/KPMI.2009.16.4.262
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- Disk type porous nickel membrane was fabricated by in-situ reduction/sintering process using compacted NiO/PMMA (PMMA; Polymethyl methacrylate) mixture at 800°C in hydrogen atmosphere. The porosity (49sim58%) of these membrane was investigated as an amount of PMMA additive. The thermal decomposition and reduction behavior of NiO/PMMA were analyzed by TG/DTA in hydrogen atmosphere and the activation energy for the hydrogen reduction of NiO and thermal degradation of PMMA was calculated as 61.1 kJ/mol, evaluated by Kissinger method. Finally, the filtering performance and pressure drop were measured by particle counting system.
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