- Spark Plasma Sintering Behaviors of M-type Barium Hexaferrite Nano Powders
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Im Doo Jung, Youngmoo Kim, Yang-Ki Hong, Seong Jin Park
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J Korean Powder Metall Inst. 2014;21(4):256-259. Published online August 1, 2014
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DOI: https://doi.org/10.4150/KPMI.2014.21.4.256
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Abstract
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A magnetic powder, M-type barium hexaferrite (BaFe12O19), was consolidated with the spark plasma sintering process. Three different holding temperatures, 850°C, 875°C and 900°C were applied to the spark plasma sintering process with the same holding times, heating rates and compaction pressure of 30 MPa. The relative density was measured simultaneously with spark plasma sintering and the convergent relative density after cooling was found to be proportional to the holding temperature. The full relative density was obtained at 900°C and the total sintering time was only 33.3 min, which was much less than the conventional furnace sintering method. The higher holding temperature also led to the higher saturation magnetic moment (σs) and the higher coercivity (Hc) in the vibrating sample magnetometer measurement. The saturation magnetic moment (σs) and the coercivity (Hc) obtained at 900°C were 56.3 emu/g and 541.5 Oe for each.
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