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[Korean]
Fabrication and Microstructure/Properties of Bulk-type Tantalum Material by a Kinetic Spray Process
Ji-Hye Lee, Ji-Won Kim, Kee-Ahn Lee
J Korean Powder Metall Inst. 2016;23(1):8-14.   Published online February 1, 2016
DOI: https://doi.org/10.4150/KPMI.2016.23.1.8
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AbstractAbstract PDF

A bulk-type Ta material is fabricated using the kinetic spray process and its microstructure and physical properties are investigated. Ta powder with an angular size in the range 9-37 μm (purity 99.95%) is sprayed on a Cu plate to form a coating layer. As a result, ~7 mm-sized bulk-type high-density material capable of being used as a sputter material is fabricated. In order to assess the physical properties of the thick coating layer at different locations, the coating material is observed at three different locations (surface, center, and interface). Furthermore, a vacuum heat treatment is applied to the coating material to reduce the variation of physical properties at different locations of the coating material and improve the density. OM, Vickers hardness test, SEM, XRD, and EBSD are implemented for analyzing the microstructure and physical properties. The fabricated Ta coating material produces porosity of 0.11~0.12%, hardness of 311~327 Hv, and minor variations at different locations. In addition, a decrease in the porosity and hardness is observed at different locations upon heat treatment.

Citations

Citations to this article as recorded by  
  • Sintering Behavior and Microstructures of Tantalum and Tantalum-Tungsten Alloys Powders
    Youngmoo Kim, Sung Ho Yang, Seong Lee, Sung Ho Lee, Joon-Woong Noh
    Journal of Korean Powder Metallurgy Institute.2020; 27(5): 373.     CrossRef
  • Manufacturing of Large-Scale Cold-Sprayed Ta Target Material and Its Sputtering Property
    Gi-Su Ham, Dong-Yeol Wi, Jun-Mo Yang, Kee-Ahn Lee
    Journal of Thermal Spray Technology.2019; 28(8): 1974.     CrossRef
  • Mechanical properties of Mo-Nb-Si-B quaternary alloy fabricated by powder metallurgical method
    Jong Min Byun, Su-Ryong Bang, Se Hoon Kim, Won June Choi, Young Do Kim
    International Journal of Refractory Metals and Hard Materials.2017; 65: 14.     CrossRef

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