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2 "Suspension plasma spray"
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Effect of Deposition Parameter and Mixing Process of Raw Materials on the Phase and Structure of Ytterbium Silicate Environmental Barrier Coatings by Suspension Plasma Spray Method
Ho-lim Ryu, Seon-A Choi, Sung-Min Lee, Yoon-Soo Han, Kyun Choi, Sahn Nahm, Yoon-Suk Oh
J Korean Powder Metall Inst. 2017;24(6):437-443.   Published online December 1, 2017
DOI: https://doi.org/10.4150/KPMI.2017.24.6.437
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SiC-based composite materials with light weight, high durability, and high-temperature stability have been actively studied for use in aerospace and defense applications. Moreover, environmental barrier coating (EBC) technologies using oxide-based ceramic materials have been studied to prevent chemical deterioration at a high temperature of 1300°C or higher. In this study, an ytterbium silicate material, which has recently been actively studied as an environmental barrier coating because of its high-temperature chemical stability, is fabricated on a sintered SiC substrate. Yb2O3 and SiO2 are used as the raw starting materials to form ytterbium disilicate (Yb2Si2O7). Suspension plasma spraying is applied as the coating method. The effect of the mixing method on the particle size and distribution, which affect the coating formation behavior, is investigated using a scanning electron microscope (SEM), an energy dispersive spectrometer (EDS), and X-ray diffraction (XRD) analysis. It is found that the originally designed compounds are not effectively formed because of the refinement and vaporization of the raw material particles, i.e., SiO2, and the formation of a porous coating structure. By changing the coating parameters such as the deposition distance, it is found that a denser coating structure can be formed at a closer deposition distance.

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  • Fabrication, Microstructure and Adhesive Properties of BCuP-5 Filler Metal/Ag Plate Composite by using Plasma Spray Process
    Seong-June Youn, Young-Kyun Kim, Jae-Sung Park, Joo-Hyun Park, Kee-Ahn Lee
    Journal of Korean Powder Metallurgy Institute.2020; 27(4): 333.     CrossRef
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Fabrication and Characterization of Ceramics and Thermal Barrier Coatings of Lanthanum Zirconate with Reduced Rare-earth Contents in the La2O3-ZrO2 System
Chang-Sup Kwon, Sujin Lee, Sung-Min Lee, Yoon-Suk Oh, Hyung-Tae Kim, Byung-Koog Jang, Seongwon Kim
J Korean Powder Metall Inst. 2015;22(6):413-419.   Published online December 1, 2015
DOI: https://doi.org/10.4150/KPMI.2015.22.6.413
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Lanthanum zirconate, La2Zr2O7, is one of the most promising candidates for next-generation thermal barrier coating (TBC) applications in high efficient gas turbines due to its low thermal conductivity and chemical stability at high temperature. In this study, bulk specimens and thermal barrier coatings are fabricated via a variety of sintering processes as well as suspension plasma spray in lanthanum zirconates with reduced rare-earth contents. The phase formation, microstructure, and thermo-physical properties of these oxide ceramics and coatings are examined. In particular, lanthanum zirconates with reduced rare-earth contents in a La2Zr2O7-4YSZ composite system exhibit a single phase of fluorite or pyrochlore after fabricated by suspension plasma spray or spark plasma sintering. The potential of lanthanum zirconate ceramics for TBC applications is also discussed.

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  • Phase Formation and Thermo-physical Properties of Lanthanum/Gadolinium Zirconate with Reduced Rare-earth Contents for Thermal Barrier Coatings
    Sujin Lee, Chang-Sup Kwon, Sung-Min Lee, Yoon-Suk Oh, Hyung-Tae Kim, Sahn Nahm, Seongwon Kim
    Journal of Korean Powder Metallurgy Institute.2015; 22(6): 420.     CrossRef

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