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HOME > J Korean Powder Metall Inst > Volume 17(3); 2010 > Article
화학적 기상 응축(CVC)법을 이용한 철-몰리브덴합금 나노 입자와 와이어의 제조
하종근, 조권구, 김기원, 류광선
Fabrication of Iron-Molybdenum Alloyed Nanoparticle and Nanowire using Chemical Vapor Condensation(CVC)
Jong-Keun Ha, Kwon-Koo Cho, Ki-Won Kim, Kwang-Sun Ryu
Journal of Korean Powder Metallurgy Institute 2010;17(3):223-229
DOI: https://doi.org/10.4150/KPMI.2010.17.3.223
1경상대학교 나노.신소재 공학부, i-큐브 센터
2경상대학교 나노.신소재 공학부, i-큐브 센터
3경상대학교 나노.신소재 공학부, i-큐브 센터
4울산대학교 화학과
1School of Materials Science and Engineering, i-cube Center & ERI, Gyeongsang National University
2School of Materials Science and Engineering, i-cube Center & ERI, Gyeongsang National University
3School of Materials Science and Engineering, i-cube Center & ERI, Gyeongsang National University
4Department of Chemistry, University of Ulsan
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Iron(Fe)-Molybdenum(Mo) alloyed nanoparticles and nanowires were produced by the chemical vapor condensation(CVC) process using the pyrolysis of iron pentacarbonyl(Fe(CO)_5) and Molybdenum hexacarbonyl(Mo(CO)_6). The influence of CVC parameter on the formation of nanoparticle, nanowire and size control was studied. The size of Fe-Mo alloyed nanoparticles can be controlled by quantity of gas flow. Also, Fe-Mo alloyed nanowires were produced by control of the work chamber pressure. Moreover, we investigated close correlation of size and morphology of Fe-Mo nanoparticles and nanowires with atomic quantity of inflow precursor into the electric furnace as the quantitative analysis. Obtained nanoparticles and nanowires were investigated by field emission scanning electron microscopy, energy dispersive spectroscopy and X-ray diffraction.

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