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- 신 열환원 공정에 의한 초미립 티타늄 카바이드 분말 합성
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- Synthesis of Ultrafine Titanium Carbide Powder by Novel Thermo-Reduction Process
- Alexandrovskii S.V.
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Journal of Korean Powder Metallurgy Institute 2003;10(6):390-394
DOI: https://doi.org/10.4150/KPMI.2003.10.6.390
Nano P/M Group, Department of Materials Technology, Korea Institute of Machinery and Materials (KIMM)
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Abstract
Ultra fine titanium carbide particles were synthesized by novel metallic thermo-reduction process. The vaporized TiC1_4+CCl_4 gases were reacted with liquid magnesium and the fine titanium carbide particles were then produced by combining the released titanium and carbon atoms. The vacuum treatment was followed to remove the residual phases of MgC1_2 and excess Mg. The stoichiometry, microstructure, fixed and carbon contents and lattice parameter were investigated in titanium carbide powders produced in various reaction parameters.
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