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Debinding Process Using Supercritical Fluids in Metal Powder Injection Molding
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HOME > J Korean Powder Metall Inst > Volume 10(1); 2003 > Article
분말사출성형에서 초임계유체를 이용한 탈지공정
Debinding Process Using Supercritical Fluids in Metal Powder Injection Molding
Journal of Korean Powder Metallurgy Institute 2003;10(1):6-14
DOI: https://doi.org/10.4150/KPMI.2003.10.1.006
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The purpose of the present study is to investigate the method decreasing debinding time as well as lowering operation condition than pure supercritical CO_2 debinding by using cosolvent or binary mixture of propane + CO_2. First method is to add cosolvent, such as n-hexane, DCM, methanol, 1-butanol, in supercritical CO_2. In case of adding cosolvent, we were found the addition of non-polar cosolvent (n-hexane) improves dramatically the binder removal rate (more than 2 times) compared with pure supercritical CO_2 debinding, second method is to use mixture of supercritical propane + CO_2, as solvent. In case of using mixture of supercritical propane + CO_2, the rate of debinding speeded up with increasing of pressure and concentration of propane at 348.15 K. It was found that addition of cosolvent (e.g., n-hexane, DCM) and binary mixture propane + CO_2 for supercritical solvent remarkably improved binder removal rate for the paraffin wax-based binder system, in comparison with using pure supercritical CO_2.

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