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Phase Developments and Microstructure Changes of Calcium Phosphate Powders Synthesized by Recycling Eggshell
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HOME > J Korean Powder Metall Inst > Volume 11(5); 2004 > Article
달걀껍질의 재 사용에 의해 제조 된 생체용 Calcium Phosphate 분말의 상변화 거동 및 미세구조 변화에 관한 연구
이상진, 김주원
Phase Developments and Microstructure Changes of Calcium Phosphate Powders Synthesized by Recycling Eggshell
Sang-Jin Lee, Joo-Won Kim
Journal of Korean Powder Metallurgy Institute 2004;11(5):391-398
DOI: https://doi.org/10.4150/KPMI.2004.11.5.391
1국립목포대학교 신소재공학
2국립목포대학교 신소재공학
1Dept. of Advanced Materials Science and Engineering, Mokpo National University
2Dept. of Advanced Materials Science and Engineering, Mokpo National University
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Calcium phosphate powders were successfully synthesized by using re-cycled eggshell and phosphoric acid. The crystallization behavior and powder morphologies of the synthesized powders were dependent on the starting condition of the eggshell, the mixing ratio and method of the eggshell and phosphoric acid, and calcination temperature. In general, beta-tricalcium phosphate was stably synthesized at about 900°C for 1h at each proper mixing ratio. And, the synthesized powders showed the similar microstructures to the morphology of original eggshell with uniform particle sizes. In this study, the calcium phosphate powders were synthesized with eggshell in various processing method. And their unique microstructures obtained from the eggshell were also. observed. The crystalline developments and microstructures of the synthesized powders were examined by X-ray diffractometer and scanning electron microscopy.


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