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The Microstructural Properties Change Owing to the Sintering Condition of T42 High Speed Steel Produced by Powder Injection Molding Process
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HOME > J Korean Powder Metall Inst > Volume 17(4); 2010 > Article
분말 사출 성형법으로 제조된 T42 고속도 공구강의 소결 조건에 따른 조직 특성 변화
도경록, 최성현, 권영삼, 조권구, 안인섭
The Microstructural Properties Change Owing to the Sintering Condition of T42 High Speed Steel Produced by Powder Injection Molding Process
Kyoung-Rok Do, Sung-Hyun Choi, Young-Sam Kwon, Kwon-Koo Cho, In-Shup Ahn
Journal of Korean Powder Metallurgy Institute 2010;17(4):312-318
DOI: https://doi.org/10.4150/KPMI.2010.17.4.312
1국립 경상대학교 나노.신소재공학부 금속재료공학과
2국립 경상대학교 나노.신소재공학부 금속재료공학과
3(주)쎄타텍
4국립 경상대학교 나노.신소재공학부 금속재료공학과
5국립 경상대학교 나노.신소재공학부 금속재료공학과
1School of Material Science and Engineering, i-Cube Center, Gyeongsang National University
2School of Material Science and Engineering, i-Cube Center, Gyeongsang National University
3Cetatech, Inc
4School of Material Science and Engineering, i-Cube Center, Gyeongsang National University
5School of Material Science and Engineering, i-Cube Center, Gyeongsang National University
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High speed steels (HSS) were used as cutting tools and wear parts, because of high strength, wear resistance, and hardness together with an appreciable toughness and fatigue resistance. Conventional manufacturing process for production of components with HSS was used by casting. The powder metallurgy techniques were currently developed due to second phase segregation of conventional process. The powder injection molding method (PIM) was received attention owing to shape without additional processes. The experimental specimens were manufactured with T42 HSS powders (59 vol%) and polymer (41 vol%). The metal powders were prealloyed water-atomised T42 HSS. The green parts were solvent debinded in normal n-Hexane at 60°C for 24 hours and thermal debinded at N_2-H_2 mixed gas atmosphere for 14 hours. Specimens were sintered in N_2, H_2 gas atmosphere and vacuum condition between 1200 and 1320°C. In result, polymer degradation temperatures about optimum conditions were found at 250°C and 480°C. After sintering at N_2 gas atmosphere, maximum hardness of 310Hv was observed at 1280°C. Fine and well dispersed carbide were observed at this condition. But relative density was under 90%. When sintering at H_2 gas atmosphere, relative density was observed to 94.5% at 1200°C. However, the low hardness was obtained due to decarbonization by hydrogen. In case of sintering at the vacuum of 10-5 torr at temperature of 1240°C, full density and 550Hv hardness were obtained without precipitation of MC and M_6C in grain boundary.


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