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Synthesis of Zr-Ti Alloy Powder by Magnesium Reduction
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HOME > J Korean Powder Metall Inst > Volume 18(4); 2011 > Article
마그네슘환원에 의한 지르코늄-티타늄 합금분말 합성
이동원, 박근태, 임태수, 이혜문, 유지훈
Synthesis of Zr-Ti Alloy Powder by Magnesium Reduction
Dong-Won Lee, Geun-Tae Park, Tae-Soo Lim, Hye-Moon Lee, Ji-Hun Yu
Journal of Korean Powder Metallurgy Institute 2011;18(4):359-364
DOI: https://doi.org/10.4150/KPMI.2011.18.4.359
1한국기계연구원 부설 재료연구소
2부산대학교 산학협력단
3한국기계연구원 부설 재료연구소
4한국기계연구원 부설 재료연구소
5한국기계연구원 부설 재료연구소
1Powder Technology Research Group, Korea Institute of Materials Science (KIMS)
2Institute of Research and Industry Cooperration, Pusan National University
3Powder Technology Research Group, Korea Institute of Materials Science (KIMS)
4Powder Technology Research Group, Korea Institute of Materials Science (KIMS)
5Powder Technology Research Group, Korea Institute of Materials Science (KIMS)
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Zr-Ti alloy powders were successfully synthesized by magnesium thermal reduction of metal chlorides. The evaporated and mixed gasses of ZrCl_4+TiCl_4 were injected to liquid magnesium and the chloride components were reduced by magnesium leading to the formation of MgCl_2. The released Zr and Ti atoms were then condensed to particle forms inside the mixture of liquid magnesium and magnesium chloride, which could be dissolved fully in post process by 1~5% HCl solution at room temperature. By the fraction-control of individually injected ZrCl_4 and TiCl_4 gasses, the final compositions of produced alloy powders were changed in the ranges of Zr-0 wt.%~20 wt.%Ti and their purity and particle size were about 99.4% and the level of several micrometers, respectively.

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