- Synthesis of Ultrafine Titanium Carbide Powder by Novel Thermo-Reduction Process
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Alexandrovskii S.V.
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J Korean Powder Metall Inst. 2003;10(6):390-394.
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DOI: https://doi.org/10.4150/KPMI.2003.10.6.390
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Abstract
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- Ultra fine titanium carbide particles were synthesized by novel metallic thermo-reduction process. The vaporized TiC1_4+CCl_4 gases were reacted with liquid magnesium and the fine titanium carbide particles were then produced by combining the released titanium and carbon atoms. The vacuum treatment was followed to remove the residual phases of MgC1_2 and excess Mg. The stoichiometry, microstructure, fixed and carbon contents and lattice parameter were investigated in titanium carbide powders produced in various reaction parameters.
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