Fabrication of Fe-TiC Composite by High-Energy Milling and Spark-Plasma Sintering

N.Q. Tuan; H.X. Khoa; N.H. Vieta; Y.H. Lee; B.H. Lee; J.S. Kim

doi:10.4150/KPMI.2013.20.5.338

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Fabrication of Fe-TiC Composite by High-Energy Milling and Spark-Plasma Sintering: N.Q. Tuan, H.X. Khoa, N.H. Vieta, Y.H. Lee, B.H. Lee, J.S. Kim; Journal of Korean Powder Metallurgy Institute 2013;20(5):338-344
DOI: https://doi.org/10.4150/KPMI.2013.20.5.338

¹School of Materials Science and Engineering, University of Ulsan
²School of Materials Science and Engineering, University of Ulsan
³School of Materials Science and Engineering, Hanoi University of Science and Technology
⁴School of Materials Science and Engineering, University of Ulsan
⁵School of Materials Science and Engineering, University of Ulsan
⁶School of Materials Science and Engineering, University of Ulsan

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Abstract

Fe-TiC composite was fabricated from Fe and TiC powders by high-energy milling and subsequent spark-plasma sintering. The microstructure, particle size and phase of Fe-TiC composite powders were investigated by field emission scanning electron microscopy and X-ray diffraction to evaluate the effect of milling conditions on the size and distribution of TiC particles in Fe matrix. TiC particle size decreased with milling time. The average TiC particle size of 38 nm was obtained after 60 minutes of milling at 1000 rpm. Prepared Fe-TiC powder mixture was densified by spark-plasma sintering. Sintered Fe-TiC compacts showed a relative density of 91.7~96.2%. The average TiC particle size of 150 nm was observed from the FE-SEM image. The microstructure, densification behavior, Vickers hardness, and fracture toughness of Fe-TiC sintered compact were investigated.

Keywords: Fe-TiC composite;high-energy milling;spark-plasma sintering;

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