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- 양극산화법에 의한 TiO2 나노튜브 어레이의 제조와 성장거동
- 김선민, 김기원, 류광선, 김유영, 조권구
- Fabrication and Growth Behavior of TiO2 Nanotube Arrays by Anodic Oxidation Method
- Seon-Min Kim, Ki-Won Kim, Kwang-Sun Ryu, Yoo-Young Kim, Kwon-Koo Cho
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Journal of Korean Powder Metallurgy Institute 2011;18(1):56-63
DOI: https://doi.org/10.4150/KPMI.2011.18.1.056
1경상대학교 나노.신소재 공학부, i-큐브 센터 & 공학연구원
2경상대학교 나노.신소재 공학부, i-큐브 센터 & 공학연구원
3울산대학교 화학과
4경남과학기술대학교 기계공학과
5경상대학교 나노.신소재 공학부, i-큐브 센터 & 공학연구원
1School of Materials Science and Engineering, i-cube Center & ERI, Gyeongsang National University
2School of Materials Science and Engineering, i-cube Center & ERI, Gyeongsang National University
3Department of Chemistry, University of Ulsan
4Department of Mechanical Engineering, Gyeongnam National University of Science and Technology
5School of Materials Science and Engineering, i-cube Center & ERI, Gyeongsang National University
2경상대학교 나노.신소재 공학부, i-큐브 센터 & 공학연구원
3울산대학교 화학과
4경남과학기술대학교 기계공학과
5경상대학교 나노.신소재 공학부, i-큐브 센터 & 공학연구원
1School of Materials Science and Engineering, i-cube Center & ERI, Gyeongsang National University
2School of Materials Science and Engineering, i-cube Center & ERI, Gyeongsang National University
3Department of Chemistry, University of Ulsan
4Department of Mechanical Engineering, Gyeongnam National University of Science and Technology
5School of Materials Science and Engineering, i-cube Center & ERI, Gyeongsang National University
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Abstract
Recently, TiO_2 nanotubes have considerably researched because of their novel application about photocatalysis, dye-sensitized solar cells (DSSCs), lithium ion battery, etc. In this work, self-standing TiO_2 nanotube arrays were fabricated by anodic oxidation method using pure Ti foil as a working electrode in ethylene glycole with 0.3M NH_4F + 2%H_2O. Growth behavior of TiO_2 nanotube arrays was compared according to temperature, voltage and time. The morphology, structure and crystalline of anodized TiO_2 nanotube arrays were observed by FE-SEM (field emission scanning electron microscope) and XRD (X-ray diffraction).
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