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- Cu, Zn, Sn, Se 혼합 분말의 소결특성에 미치는 볼밀링 영향
- 안종헌, 정운화, 장윤정, 이성헌, 김규호
- Effects of Ball Milling Condition on Sintering of Cu, Zn, Sn and Se Mixed Powders
- Jong-Heon Ahn, Woon-Hwa Jung, Yun-Jung Jang, Seong-Heon Lee, Kyoo-Ho Kim
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Journal of Korean Powder Metallurgy Institute 2011;18(3):256-261
DOI: https://doi.org/10.4150/KPMI.2011.18.3.256
1영남대학교 신소재공학부
2영남대학교 신소재공학부
3영남대학교 신소재공학부
4영남대학교 신소재공학부
5영남대학교 신소재공학부
1School of Materials Engineering, Yeungnam University Gyongsan
2School of Materials Engineering, Yeungnam University Gyongsan
3School of Materials Engineering, Yeungnam University Gyongsan
4School of Materials Engineering, Yeungnam University Gyongsan
5School of Materials Engineering, Yeungnam University Gyongsan
2영남대학교 신소재공학부
3영남대학교 신소재공학부
4영남대학교 신소재공학부
5영남대학교 신소재공학부
1School of Materials Engineering, Yeungnam University Gyongsan
2School of Materials Engineering, Yeungnam University Gyongsan
3School of Materials Engineering, Yeungnam University Gyongsan
4School of Materials Engineering, Yeungnam University Gyongsan
5School of Materials Engineering, Yeungnam University Gyongsan
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Abstract
In order to make a Cu_2ZnSnSe_4 (CZTSe) sputtering target sintered for solar cell application, synthesis of CZTSe compound by solid state reaction of Cu, Zn, Sn and Se mixed powders and effects of ball milling condition on sinterability such as ball size, combination of ball size, ball milling time and sintering temperature, was investigated. As a result of this research, sintering at 500°C after ball milling using mixed balls of 1 mm and 3 mm for 72 hours was the optimum condition to synthesis near stoichiometric composition of Cu_2ZnSnSe_4 and to prepare sintered pellet with high density relatively.
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