- Phase Formation and Mechanical Property of YSZ‒30 vol.% WC Composite Ceramics Fabricated by Hot Pressing
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Jin-Kwon Kim, Jae-Hyeong Choi, Nahm Sahn, Sung-Soo Ryu, Seongwon Kim
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J Powder Mater. 2023;30(5):409-414. Published online October 1, 2023
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DOI: https://doi.org/10.4150/KPMI.2023.30.5.409
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Abstract
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YSZ (Y2O3-stabilized zirconia)-based ceramics have excellent mechanical properties, such as high strength and wear resistance. In the application, YSZ is utilized in the bead mill, a fine-grinding process. YSZ-based parts, such as the rotor and pin, can be easily damaged by continuous application with high rpm in the bead mill process. In that case, adding WC particles improves the tribological and mechanical properties. YSZ-30 vol.% WC composite ceramics are manufactured via hot pressing under different pressures (10/30/60 MPa). The hot-pressed composite ceramics measure the physical properties, such as porosity and bulk density values. In addition, the phase formation of these composite ceramics is analyzed and discussed with those of physical properties. For the increased applied pressure of hot pressing, the tetragonality of YSZ and the crystallinity of WC are enhanced. The mechanical properties indicate an improved tendency with the increase in the applied pressure of hot pressing.
- Effect of Sintering Additive and Composition on Cutting Performance of SiAlON
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Jae-Hyeong Choi, Sung-Min Lee, Sahn Nahm, Seongwon Kim
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J Korean Powder Metall Inst. 2019;26(5):415-420. Published online October 1, 2019
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DOI: https://doi.org/10.4150/KPMI.2019.26.5.415
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Abstract
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SiAlON ceramics are used as ceramic cutting tools for heat-resistant super alloys (HRSAs) due to their excellent fracture toughness and thermal properties. They are manufactured from nitride and oxide raw materials. Mixtures of nitrides and oxides are densified via liquid phase sintering by using gas pressure sintering. Rare earth oxides, when used as sintering additives, affect the color and mechanical properties of SiAlON. Moreover, these sintering additives influence the cutting performance. In this study, we have prepared Ybm/3Si12-(m+n)Alm+nOnN16-n (m = 0.5; n = 0.5, 1.0) ceramics and manufactured SiAlON ceramics, which resulted in different colors. In addition, the characteristics of the sintered SiAlON ceramics such as fracture toughness and microstructure have been investigated and results of the cutting test have been analyzed.
- Phase Formation and Physical Properties of SiAlON Ceramics Fabricated by Gas-Pressure Reactive Sintering
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Soyul Lee, Jae-Hyeong Choi, Yoonsoo Han, Sung-Min Lee, Seongwon Kim
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J Korean Powder Metall Inst. 2017;24(6):431-436. Published online December 1, 2017
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DOI: https://doi.org/10.4150/KPMI.2017.24.6.431
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Abstract
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SiAlON-based ceramics are some of the most typical oxynitride ceramic materials, which can be used as cutting tools for heat-resistant super-alloys (HRSA). SiAlON can be fabricated by using gas-pressure reactive sintering from the raw materials, nitrides and oxides such as Si3N4, AlN, Al2O3, and Yb2O3. In this study, we fabricate Ybm/3Si12-(m+n)Alm+nOnN16-n (m=0.3, n=1.9, 2.3, 2.7) ceramics by using gas-pressure sintering at different sintering temperatures. Then, the densification behavior, phase formation, microstructure, and hardness of the sintered specimens are characterized. We obtain a fully densified specimen with β- SiAlON after gas-pressure sintering at 1820°C for 90 min. under 10 atm N2 pressure. These SiAlON ceramic materials exhibited hardness values of ~92.9 HRA. The potential of these SiAlON ceramics for cutting tool application is also discussed.
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