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Characterization of the Manufacturing Process and Mechanical Properties of CoCrFeMnNi High-Entropy Alloys via Metal Injection Molding and Hot Isostatic Pressing
Eun Seong Kim, Jae Man Park, Do Won Lee, Hyojeong Ha, Jungho Choe, Jaemin Wang, Seong Jin Park, Byeong-Joo Lee, Hyoung Seop Kim
J Powder Mater. 2024;31(3):243-254.   Published online June 27, 2024
DOI: https://doi.org/10.4150/jpm.2024.00059
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High-entropy alloys (HEAs) have been reported to have better properties than conventional materials; however, they are more expensive due to the high cost of their main components. Therefore, research is needed to reduce manufacturing costs. In this study, CoCrFeMnNi HEAs were prepared using metal injection molding (MIM), which is a powder metallurgy process that involves less material waste than machining process. Although the MIM-processed samples were in the face-centered cubic (FCC) phase, porosity remained after sintering at 1200°C, 1250°C, and 1275°C. In this study, the hot isostatic pressing (HIP) process, which considers both temperature (1150°C) and pressure (150 MPa), was adopted to improve the quality of the MIM samples. Although the hardness of the HIP-treated samples decreased slightly and the Mn composition was significantly reduced, the process effectively eliminated many pores that remained after the 1275°C MIM process. The HIP process can improve the quality of the alloy.
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Fabrication of Equiatomic CoCrFeMnNi High-Entropy Alloy by Metal Injection Molding Process Using Coarse-Sized Powders
Eun Seong Kim, Jae Man Park, Ji Sun Lee, Jungho Choe, Soung Yeoul Ahn, Sang Guk Jeong, Do Won Lee, Seong Jin Park, Hyoung Seop Kim
J Powder Mater. 2023;30(1):1-6.   Published online February 1, 2023
DOI: https://doi.org/10.4150/KPMI.2023.30.1.1
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  • 1 Citations
AbstractAbstract PDF

High-entropy alloys (HEAs) are attracting attention because of their excellent properties and functions; however, they are relatively expensive compared with commercial alloys. Therefore, various efforts have been made to reduce the cost of raw materials. In this study, MIM is attempted using coarse equiatomic CoCrFeMnNi HEA powders. The mixing ratio (powder:binder) for HEA feedstock preparation is explored using torque rheometer. The block-shaped green parts are fabricated through a metal injection molding process using feedstock. The thermal debinding conditions are explored by thermogravimetric analysis, and solvent and thermal debinding are performed. It is densified under various sintering conditions considering the melting point of the HEA. The final product, which contains a small amount of non-FCC phase, is manufactured at a sintering temperature of 1250°C.

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  • Characterization of the Manufacturing Process and Mechanical Properties of CoCrFeMnNi High-Entropy Alloys via Metal Injection Molding and Hot Isostatic Pressing
    Eun Seong Kim, Jae Man Park, Do Won Lee, Hyojeong Ha, Jungho Choe, Jaemin Wang, Seong Jin Park, Byeong-Joo Lee, Hyoung Seop Kim
    journal of Korean Powder Metallurgy Institute.2024; 31(3): 243.     CrossRef

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