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Investigation on Microstructure and Flowability of Gas Atomized Heat-resistant KHR45A Alloy Powders for Additive Manufacturing
Geonwoo Baek, Mohsen Saboktakin Rizi, Yeeun Lee, SungJae Jo, Joo-Hyun Choi, Soon-Jik Hong
J Powder Mater. 2023;30(1):13-21.   Published online February 1, 2023
DOI: https://doi.org/10.4150/KPMI.2023.30.1.13
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  • 1 Citations
AbstractAbstract PDF

In additive manufacturing, the flowability of feedstock particles determines the quality of the parts that are affected by different parameters, including the chemistry and morphology of the powders and particle size distribution. In this study, the microstructures and flowabilities of gas-atomized heat-resistant alloys for additive manufacturing applications are investigated. A KHR45A alloy powder with a composition of Fe-30Cr-40Mn-1.8Nb (wt.%) is fabricated using gas atomization process. The microstructure and effect of powder chemistry and morphology on the flow behavior are investigated by scanning electron microscopy (SEM), X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), and revolution powder analysis. The results reveal the formation of spherical particles composed of single-phase FCC dendritic structures after gas atomization. SEM observations show variations in the microstructures of the powder particles with different size distributions. Elemental distribution maps, line scans, and high-resolution XPS results indicate the presence of a Si-rich oxide accompanied by Fe, Cr, and Nb metal oxides in the outer layer of the powders. The flowability behavior is found to be induced by the particle size distribution, which can be attributed to the interparticle interactions and friction of particles with different sizes.

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  • Al-based amorphous coatings by warm spraying: Numerical simulation and experimental validation
    Deming Wang, Nianchu Wu, Peng Cao
    Journal of Alloys and Compounds.2024; 1008: 176674.     CrossRef
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Improving Flow Property of AlSi10Mg Powder for Additive Manufacturing via Surface Treatment using Methyltrichlorosilane
Sang Cheol Park, In Yeong Kim, Young Il Kim, Dae-Kyeom Kim, Kee-Ahn Lee, Soong Ju Oh, Bin Lee
J Powder Mater. 2022;29(5):363-369.   Published online October 1, 2022
DOI: https://doi.org/10.4150/KPMI.2022.29.5.363
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  • 1 Citations
AbstractAbstract PDF

AlSi10Mg alloys are being actively studied through additive manufacturing for application in the automobile and aerospace industries because of their excellent mechanical properties. To obtain a consistently high quality product through additive manufacturing, studying the flowability and spreadability of the metal powder is necessary. AlSi10Mg powder easily forms an oxide film on the powder surface and has hydrophilic properties, making it vulnerable to moisture. Therefore, in this study, AlSi10Mg powder was hydrophobically modified through silane surface treatment to improve the flowability and spreadability by reducing the effects of moisture. The improved flowability according to the number of silane surface treatments was confirmed using a Carney flowmeter. In addition, to confirm the effects of improved spreadability, the powder prior to surface treatment and that subjected to surface treatment four times were measured and compared using s self-designed recoating tester. The results of this study confirmed the improved flowability and spreadability based on the modified metal powder from hydrophilic to hydrophobic for obtaining a highquality additive manufacturing product.

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  • Residual Stress Analysis of Additive Manufactured A356.2 Aluminum Alloys using X-Ray Diffraction Methods
    SangCheol Park, InYeong Kim, Young Il Kim, Dae-Kyeom Kim, Soong Ju Oh, Kee-Ahn Lee, Bin Lee
    Korean Journal of Metals and Materials.2023; 61(7): 534.     CrossRef
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Effect of Particle Sphericity on the Rheological Properties of Ti-6Al-4V Powders for Laser Powder Bed Fusion Process
T. Y. Kim, M. H. Kang, J. H. Kim, J.K. Hong, J.H. Yu, J.I. Lee
J Powder Mater. 2022;29(2):99-109.   Published online April 1, 2022
DOI: https://doi.org/10.4150/KPMI.2022.29.2.99
  • 369 View
  • 8 Download
  • 3 Citations
AbstractAbstract PDF

Powder flowability is critical in additive manufacturing processes, especially for laser powder bed fusion. Many powder features, such as powder size distribution, particle shape, surface roughness, and chemical composition, simultaneously affect the flow properties of a powder; however, the individual effect of each factor on powder flowability has not been comprehensively evaluated. In this study, the impact of particle shape (sphericity) on the rheological properties of Ti-6Al-4V powder is quantified using an FT4 powder rheometer. Dynamic image analysis is conducted on plasma-atomized (PA) and gas-atomized (GA) powders to evaluate their particle sphericity. PA and GA powders exhibit negligible differences in compressibility and permeability tests, but GA powder shows more cohesive behavior, especially in a dynamic state, because lower particle sphericity facilitates interaction between particles during the powder flow. These results provide guidelines for the manufacturing of advanced metal powders with excellent powder flowability for laser powder bed fusion.

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  • Enhanced Microstructure and Wear Resistance of Ti–6Al–4V Alloy with Vanadium Carbide Coating via Directed Energy Deposition
    Ui Jun Ko, Ju Hyeong Jung, Jung Hyun Kang, Kyunsuk Choi, Jeoung Han Kim
    Materials.2024; 17(3): 733.     CrossRef
  • Microstructural Evolution and Mechanical Properties of Ti-6Al-4V Alloy through Selective Laser Melting: Comprehensive Study on the Effect of Hot Isostatic Pressing (HIP)
    Gargi Roy, Raj Narayan Hajra, Woo Hyeok Kim, Jongwon Lee, Sangwoo Kim, Jeoung Han Kim
    journal of Korean Powder Metallurgy Institute.2024; 31(1): 1.     CrossRef
  • Cryogenic Tensile Behavior of Ferrous Medium-entropy Alloy Additively Manufactured by Laser Powder Bed Fusion
    Seungyeon Lee, Kyung Tae Kim, Ji-Hun Yu, Hyoung Seop Kim, Jae Wung Bae, Jeong Min Park
    journal of Korean Powder Metallurgy Institute.2024; 31(1): 8.     CrossRef
Review Paper
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Review on Characterization Method and Recent Research Trend about Metal Powder for Powder Bed Fusion (PBF) Process
Bin Lee, Dae-Kyeom Kim, Young Il Kim, Do Hoon Kim, Yong Son, Kyoung-Tae Park, Taek-Soo Kim
J Korean Powder Metall Inst. 2020;27(6):509-519.   Published online December 1, 2020
DOI: https://doi.org/10.4150/KPMI.2020.27.6.509
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  • 4 Citations
AbstractAbstract PDF

A well-established characterization method is required in powder bed fusion (PBF) metal additive manufacturing, where metal powder is used. The characterization methods from the traditional powder metallurgy process are still being used. However, it is necessary to develop advanced methods of property evaluation with the advances in additive manufacturing technology. In this article, the characterization methods of powders for metal PBF are reviewed, and the recent research trends are introduced. Standardization status and specifications for metal powder for the PBF process which published by the ISO, ASTM, and MPIF are also covered. The establishment of powder characterization methods are expected to contribute to the metal powder industry and the advancement of additive manufacturing technology through the creation of related databases.

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  • A Study on Fabrication of PCD Endmill Holder using PBF Additive Manufacturing Technology
    Min-Woo Sa, Ho-Min Son, Kyung-Hwan Park, Sang-Geun Lee, Dae-Ho Shin, Dong-Gyu Kim
    Journal of the Korean Society of Manufacturing Process Engineers.2024; 23(6): 124.     CrossRef
  • Rheological Characteristic Analysis Methods and Tests of Metal Powders for PBF Additive Manufacturing
    Wan-Sik Woo, Ho-Jin Lee
    Journal of the Korean Society of Manufacturing Process Engineers.2023; 22(10): 1.     CrossRef
  • Residual Stress Analysis of Additive Manufactured A356.2 Aluminum Alloys using X-Ray Diffraction Methods
    SangCheol Park, InYeong Kim, Young Il Kim, Dae-Kyeom Kim, Soong Ju Oh, Kee-Ahn Lee, Bin Lee
    Korean Journal of Metals and Materials.2023; 61(7): 534.     CrossRef
  • Enhancing spreadability of hydrogenation-dehydrogenation titanium powder and novel method to characterize powder spreadability for powder bed fusion additive manufacturing
    Young Il Kim, Dae-Kyeom Kim, InYeong Kim, Sang Cheol Park, Dongju Lee, Bin Lee
    Materials & Design.2022; 223: 111247.     CrossRef

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