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5 "Hot isostatic pressing"
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Characterization of the Manufacturing Process and Mechanical Properties of CoCrFeMnNi High-Entropy Alloys via Metal Injection Molding and Hot Isostatic Pressing
Eun Seong Kim, Jae Man Park, Do Won Lee, Hyojeong Ha, Jungho Choe, Jaemin Wang, Seong Jin Park, Byeong-Joo Lee, Hyoung Seop Kim
J Powder Mater. 2024;31(3):243-254.   Published online June 27, 2024
DOI: https://doi.org/10.4150/jpm.2024.00059
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High-entropy alloys (HEAs) have been reported to have better properties than conventional materials; however, they are more expensive due to the high cost of their main components. Therefore, research is needed to reduce manufacturing costs. In this study, CoCrFeMnNi HEAs were prepared using metal injection molding (MIM), which is a powder metallurgy process that involves less material waste than machining process. Although the MIM-processed samples were in the face-centered cubic (FCC) phase, porosity remained after sintering at 1200°C, 1250°C, and 1275°C. In this study, the hot isostatic pressing (HIP) process, which considers both temperature (1150°C) and pressure (150 MPa), was adopted to improve the quality of the MIM samples. Although the hardness of the HIP-treated samples decreased slightly and the Mn composition was significantly reduced, the process effectively eliminated many pores that remained after the 1275°C MIM process. The HIP process can improve the quality of the alloy.
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Effect of Hot Isostatic Pressing on the Stellite 6 Alloy prepared by Directed Energy Deposition
Joowon Suh, Jae Hyeon Koh, Young-Bum Chun, Young Do Kim, Jinsung Jang, Suk Hoon Kang, Heung Nam Han
J Powder Mater. 2024;31(2):152-162.   Published online April 30, 2024
DOI: https://doi.org/10.4150/jpm.2024.00066
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The directed energy deposited (DED) alloys show higher hardness values than the welded alloys due to the finer microstructure following the high cooling rate. However, defects such as microcracks, pores, and the residual stress are remained within the DED alloy. These defects deteriorate the wear behavior so post-processing such as heat treatment and hot isostatic pressing (HIP) are applied to DED alloys to reduce the defects. HIP was chosen in this study because the high pressure and temperature uniformly reduced the defects. The HIP is processed at 1150oC under 100 MPa for 4 hours. After HIP, microcracks are disappeared and porosity is reduced by 86.9%. Carbides are spherodized due to the interdiffusion of Cr and C between the dendrite and interdendrite region. After HIP, the nanohardness (GPa) of carbides increased from 11.1 to 12, and the Co matrix decreased from 8.8 to 7.9. Vickers hardness (HV) decreased by 18.9 % after HIP. The dislocation density (10-2/m2) decreased from 7.34 to 0.34 and the residual stress (MPa) changed from tensile 79 to a compressive -246 by HIP. This study indicates that HIP is effective in reducing defects, and the HIP DED Stellite 6 exhibits a higher HV than welded Stellite 6.
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Microstructural Evolution and Mechanical Properties of Ti-6Al-4V Alloy through Selective Laser Melting: Comprehensive Study on the Effect of Hot Isostatic Pressing (HIP)
Gargi Roy, Raj Narayan Hajra, Woo Hyeok Kim, Jongwon Lee, Sangwoo Kim, Jeoung Han Kim
J Powder Mater. 2024;31(1):1-7.   Published online February 28, 2024
DOI: https://doi.org/10.4150/KPMI.2024.31.1.1
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  • 1 Citations
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This study explores the profound impact of varying oxygen content on microstructural and mechanical properties in specimens HO and LO. The higher oxygen concentration in specimen HO is found to significantly influence alpha lath sizes, resulting in a size of 0.5-1 μm, contrasting with the 1-1.5 μm size observed in specimen LO. Pore fraction, governed by oxygen concentration, is high in specimen HO, registering a value of 0.11%, whereas specimen LO exhibits a lower pore fraction (0.02%). Varied pore types in each specimen further underscore the role of oxygen concentration in shaping microstructural morphology. Despite these microstructural variations, the average hardness remains consistent at ~370 HV. This study emphasizes the pivotal role of oxygen content in influencing microstructural features, contributing to a comprehensive understanding of the intricate interplay between elemental composition and material properties.

Citations

Citations to this article as recorded by  
  • Mechanical response and microstructural evolution of a composite joint fabricated by green laser dissimilar welding of VCoNi medium entropy alloy and 17-4PH stainless steel
    Hadiseh Esmaeilpoor, Mahdi Aghaahmadi, Hyun Jong Yoo, Chan Woong Park, Tae Jin Jang, Seok Su Sohn, Jeoung Han Kim
    Journal of Materials Science & Technology.2025; 213: 223.     CrossRef
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Enhancement of Thermoelectric Performance in Spark Plasma Sintered p-Type Bi0.5Sb1.5Te3.0 Compound via Hot Isostatic Pressing (HIP) Induced Reduction of Lattice Thermal Conductivity
Soo-Ho Jung, Ye Jin Woo, Kyung Tae Kim, Seungki Jo
J Powder Mater. 2023;30(2):123-129.   Published online April 1, 2023
DOI: https://doi.org/10.4150/KPMI.2023.30.2.123
  • 466 View
  • 3 Download
  • 3 Citations
AbstractAbstract PDF

High-temperature and high-pressure post-processing applied to sintered thermoelectric materials can create nanoscale defects, thereby enhancing their thermoelectric performance. Here, we investigate the effect of hot isostatic pressing (HIP) as a post-processing treatment on the thermoelectric properties of p-type Bi0.5Sb1.5Te3.0 compounds sintered via spark plasma sintering. The sample post-processed via HIP maintains its electronic transport properties despite the reduced microstructural texturing. Moreover, lattice thermal conductivity is significantly reduced owing to activated phonon scattering, which can be attributed to the nanoscale defects created during HIP, resulting in an ~18% increase in peak zT value, which reaches ~1.43 at 100°C. This study validates that HIP enhances the thermoelectric performance by controlling the thermal transport without having any detrimental effects on the electronic transport properties of thermoelectric materials.

Citations

Citations to this article as recorded by  
  • Exploring Thermoelectric Transport Properties and Band Parameters of n-Type Bi2-xSbxTe3 Compounds Using the Single Parabolic Band Model
    Linh Ba Vu, Soo-ho Jung, Jinhee Bae, Jong Min Park, Kyung Tae Kim, Injoon Son, Seungki Jo
    journal of Korean Powder Metallurgy Institute.2024; 31(2): 119.     CrossRef
  • Investigation of the Thermal-to-Electrical Properties of Transition Metal-Sb Alloys Synthesized for Thermoelectric Applications
    Jong Min Park, Seungki Jo, Sooho Jung, Jinhee Bae, Linh Ba Vu, Kwi-Il Park, Kyung Tae Kim
    journal of Korean Powder Metallurgy Institute.2024; 31(3): 236.     CrossRef
  • Enhancing Electrical Properties of N-type Bismuth Telluride Alloys through Graphene Oxide Incorporation in Extrusion 3D Printing
    Jinhee Bae, Seungki Jo, Kyung Tae Kim
    journal of Korean Powder Metallurgy Institute.2023; 30(4): 318.     CrossRef
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Effect of Hot Isostatic Pressing on the Microstructure and Properties of Kinetic Sprayed Nb Coating Material
Ji-Hye Lee, Sangsun Yang, Kee-Ahn Lee
J Korean Powder Metall Inst. 2016;23(1):15-20.   Published online February 1, 2016
DOI: https://doi.org/10.4150/KPMI.2016.23.1.15
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Niobium is one of the most important and rarest metals, and is used in the electronic and energy industries. However, it’s extremely high melting point and oxygen affinity limits the manufacture of Nb coating materials. Here, a Nb coating material is manufactured using a kinetic spray process followed by hot isotactic pressing to improve its properties. OM (optical microscope), XRD (X-ray diffraction), SEM (scanning electron microscopy), and Vickers hardness and EPMA (electron probe micro analyzer) tests are employed to investigate the macroscopic properties of the manufactured Nb materials. The powder used to manufacture the material has angular-shaped particles with an average particle size of 23.8 μm. The porosity and hardness of the manufactured Nb material are 0.18% and 221 Hv, respectively. Additional HIP is applied to the manufactured Nb material for 4 h under an Ar atmosphere after which the porosity decreases to 0.08% and the hardness increases to 253 Hv. Phase analysis after the HIP shows the presence of only pure Nb. The study also discusses the possibility of using the manufactured Nb material as a sputtering target.


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