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Effect of Sintering Temperature on the Microstructure and Mechanical Properties of Solid Oxide Fuel Cell Anode Fabricated by Spark Plasma Sintering
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HOME > J Powder Mater > Volume 20(6); 2013 > Article
플라즈마 소결법을 이용한 고체산화물 연료전지 음극 제조 시 소결온도에 따른 미세구조 및 물성평가
송병주, 김가람, 김혜성
Effect of Sintering Temperature on the Microstructure and Mechanical Properties of Solid Oxide Fuel Cell Anode Fabricated by Spark Plasma Sintering
Byung Ju Song, Ka Ram Kim, Hye Sung Kim
Journal of Powder Materials 2013;20(6):425-431
DOI: https://doi.org/10.4150/KPMI.2013.20.6.425
1부산대학교 나노융합기술학과
2부산대학교 나노융합기술학과
3부산대학교 나노융합기술학과
1Department of Nano Fusion Technology, College of Nanoscience & Nanotechnology, Pusan National University
2Department of Nano Fusion Technology, College of Nanoscience & Nanotechnology, Pusan National University
3Department of Nano Fusion Technology, College of Nanoscience & Nanotechnology, Pusan National University
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Microstructural and mechanical properties of Ni-YSZ fabricated using SPS processing have been investigated at various sintering temperatures. Our study shows samples to be applied as a SOFC anode have the proper porosity of 40% and high hardness when processed at 1100°C. These results are comparable to the values obtained at 100-200°C higher sintering temperature reported by others. This result is important because when the fabrication processes are performed above 1100°C, the mechanical property starts to decrease drastically. This is caused by the fast grain coarsening at the higher temperature, which initiates a mismatch between thermal expansion coefficients of Ni and YSZ and induces cracks as well.


Journal of Powder Materials : Journal of Powder Materials