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20 "Ji-Hun Yu"
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Data-driven Approach to Explore the Contribution of Process Parameters for Laser Powder Bed Fusion of a Ti-6Al-4V Alloy
Jeong Min Park, Jaimyun Jung, Seungyeon Lee, Haeum Park, Yeon Woo Kim, Ji-Hun Yu
J Powder Mater. 2024;31(2):137-145.   Published online April 30, 2024
DOI: https://doi.org/10.4150/jpm.2024.00038
  • 785 View
  • 44 Download
AbstractAbstract PDF
In order to predict the process window of laser powder bed fusion (LPBF) for printing metallic components, the calculation of volumetric energy density (VED) has been widely calculated for controlling process parameters. However, because it is assumed that the process parameters contribute equally to heat input, the VED still has limitation for predicting the process window of LPBF-processed materials. In this study, an explainable machine learning (xML) approach was adopted to predict and understand the contribution of each process parameter to defect evolution in Ti alloys in the LPBF process. Various ML models were trained, and the Shapley additive explanation method was adopted to quantify the importance of each process parameter. This study can offer effective guidelines for fine-tuning process parameters to fabricate high-quality products using LPBF.
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Cryogenic Tensile Behavior of Ferrous Medium-entropy Alloy Additively Manufactured by Laser Powder Bed Fusion
Seungyeon Lee, Kyung Tae Kim, Ji-Hun Yu, Hyoung Seop Kim, Jae Wung Bae, Jeong Min Park
J Powder Mater. 2024;31(1):8-15.   Published online February 28, 2024
DOI: https://doi.org/10.4150/KPMI.2024.31.1.8
  • 2,023 View
  • 101 Download
  • 2 Citations
AbstractAbstract PDF

The emergence of ferrous-medium entropy alloys (FeMEAs) with excellent tensile properties represents a potential direction for designing alloys based on metastable engineering. In this study, an FeMEA is successfully fabricated using laser powder bed fusion (LPBF), a metal additive manufacturing technology. Tensile tests are conducted on the LPBF-processed FeMEA at room temperature and cryogenic temperatures (77 K). At 77 K, the LPBF-processed FeMEA exhibits high yield strength and excellent ultimate tensile strength through active deformation-induced martensitic transformation. Furthermore, due to the low stability of the face-centered cubic (FCC) phase of the LPBF-processed FeMEA based on nano-scale solute heterogeneity, stress-induced martensitic transformation occurs, accompanied by the appearance of a yield point phenomenon during cryogenic tensile deformation. This study elucidates the origin of the yield point phenomenon and deformation behavior of the FeMEA at 77 K.

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  • Cryogenic tensile behavior of carbon-doped CoCrFeMnNi high-entropy alloys additively manufactured by laser powder bed fusion
    Haeum Park, Hyeonseok Kwon, Kyung Tae Kim, Ji-Hun Yu, Jungho Choe, Hyokyung Sung, Hyoung Seop Kim, Jung Gi Kim, Jeong Min Park
    Additive Manufacturing.2024; 86: 104223.     CrossRef
  • Recent progress in high-entropy alloys for laser powder bed fusion: Design, processing, microstructure, and performance
    Asker Jarlöv, Zhiguang Zhu, Weiming Ji, Shubo Gao, Zhiheng Hu, Priyanka Vivegananthan, Yujia Tian, Devesh Raju Kripalani, Haiyang Fan, Hang Li Seet, Changjun Han, Liming Tan, Feng Liu, Mui Ling Sharon Nai, Kun Zhou
    Materials Science and Engineering: R: Reports.2024; 161: 100834.     CrossRef
Articles
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Effect of Bulk Shape on Mechanical Properties of Ti-6Al-4V Alloy Manufactured by Laser Powder Bed Fusion
Haeum Park, Yeon Woo Kim, Seungyeon Lee, Kyung Tae Kim, Ji-Hun Yu, Jung Gi Kim, Jeong Min Park
J Powder Mater. 2023;30(2):140-145.   Published online April 1, 2023
DOI: https://doi.org/10.4150/KPMI.2023.30.2.140
  • 680 View
  • 11 Download
  • 5 Citations
AbstractAbstract PDF

Although the Ti–6Al–4V alloy has been used in the aircraft industry owing to its excellent mechanical properties and low density, the low formability of the alloy hinders broadening its applications. Recently, laser-powder bed fusion (L-PBF) has become a novel process for overcoming the limitations of the alloy (i.e., low formability), owing to the high degree of design freedom for the geometry of products having outstanding performance used in hightech applications. In this study, to investigate the effect of bulk shape on the microstructure and mechanical properties of L-PBFed Ti-6Al-4V alloys, two types of samples are fabricated using L-PBF: thick and thin samples. The thick sample exhibits lower strength and higher ductility than the thin sample owing to the larger grain size and lower residual dislocation density of the thick sample because of the heat input during the L-PBF process.

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  • Cryogenic Tensile Behavior of Ferrous Medium-entropy Alloy Additively Manufactured by Laser Powder Bed Fusion
    Seungyeon Lee, Kyung Tae Kim, Ji-Hun Yu, Hyoung Seop Kim, Jae Wung Bae, Jeong Min Park
    journal of Korean Powder Metallurgy Institute.2024; 31(1): 8.     CrossRef
  • Microstructural Evolution and Mechanical Properties of Ti-6Al-4V Alloy through Selective Laser Melting: Comprehensive Study on the Effect of Hot Isostatic Pressing (HIP)
    Gargi Roy, Raj Narayan Hajra, Woo Hyeok Kim, Jongwon Lee, Sangwoo Kim, Jeoung Han Kim
    journal of Korean Powder Metallurgy Institute.2024; 31(1): 1.     CrossRef
  • Data-driven Approach to Explore the Contribution of Process Parameters for Laser Powder Bed Fusion of a Ti-6Al-4V Alloy
    Jeong Min Park, Jaimyun Jung, Seungyeon Lee, Haeum Park, Yeon Woo Kim, Ji-Hun Yu
    journal of Korean Powder Metallurgy Institute.2024; 31(2): 137.     CrossRef
  • A Parametric Study on the L-PBF Process of an AlSi10Mg Alloy for High-Speed Productivity of Automotive Prototype Parts
    Yeonha Chang, Hyomoon Joo, Wanghyun Yong, Yeongcheol Jo, Seongjin Kim, Hanjae Kim, Yeon Woo Kim, Kyung Tae Kim, Jeong Min Park
    Journal of Powder Materials.2024; 31(5): 390.     CrossRef
  • High-speed manufacturing-driven strength-ductility improvement of H13 tool steel fabricated by selective laser melting
    Yeon Woo Kim, Haeum Park, Young Seong Eom, Dong Gill Ahn, Kyung Tae Kim, Ji-hun Yu, Yoon Suk Choi, Jeong Min Park
    Powder Metallurgy.2023; 66(5): 582.     CrossRef
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Effect of Substrate Pre-heating on Microstructure and Magnetic Properties of Nd-Fe-B Permanent Magnet Manufactured by L-PBF
Yeon Woo Kim, Haeum Park, Tae-Hoon Kim, Kyung Tae Kim, Ji-Hun Yu, Yoon Suk Choi, Jeong Min Park
J Powder Mater. 2023;30(2):116-122.   Published online April 1, 2023
DOI: https://doi.org/10.4150/KPMI.2023.30.2.116
  • 136 View
  • 4 Download
AbstractAbstract PDF

Because magnets fabricated using Nd-Fe-B exhibit excellent magnetic properties, this novel material is used in various high-tech industries. However, because of the brittleness and low formability of Nd-Fe-B magnets, the design freedom of shapes for improving the performance is limited based on conventional tooling and postprocessing. Laserpowder bed fusion (L-PBF), the most famous additive manufacturing (AM) technique, has recently emerged as a novel process for producing geometrically complex shapes of Nd-Fe-B parts owing to its high precision and good spatial resolution. However, because of the repeated thermal shock applied to the materials during L-PBF, it is difficult to fabricate a dense Nd-Fe-B magnet. In this study, a high-density (>96%) Nd-Fe-B magnet is successfully fabricated by minimizing the thermal residual stress caused by substrate heating during L-PBF.

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Characterization and Classification of Pores in Metal 3D Printing Materials with X-ray Tomography and Machine Learning
Eun-Ah Kim, Se-Hun Kwon, Dong-Yeol Yang, Ji-Hun Yu, Kwon-Ill Kim, Hak-Sung Lee
J Korean Powder Metall Inst. 2021;28(3):208-215.   Published online June 1, 2021
DOI: https://doi.org/10.4150/KPMI.2021.28.3.208
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AbstractAbstract PDF

Metal three-dimensional (3D) printing is an important emerging processing method in powder metallurgy. There are many successful applications of additive manufacturing. However, processing parameters such as laser power and scan speed must be manually optimized despite the development of artificial intelligence. Automatic calibration using information in an additive manufacturing database is desirable. In this study, 15 commercial pure titanium samples are processed under different conditions, and the 3D pore structures are characterized by X-ray tomography. These samples are easily classified into three categories, unmelted, well melted, or overmelted, depending on the laser energy density. Using more than 10,000 projected images for each category, convolutional neural networks are applied, and almost perfect classification of these samples is obtained. This result demonstrates that machine learning methods based on X-ray tomography can be helpful to automatically identify more suitable processing parameters.

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Additive Manufacturing for Sensor Integrated Components
Im Doo Jung, Min Sik Lee, Young Jin Woo, Kyung Tae Kim, Ji-Hun Yu
J Korean Powder Metall Inst. 2020;27(2):111-118.   Published online April 1, 2020
DOI: https://doi.org/10.4150/KPMI.2020.27.2.111
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AbstractAbstract PDF

The convergence of artificial intelligence with smart factories or smart mechanical systems has been actively studied to maximize the efficiency and safety. Despite the high improvement of artificial neural networks, their application in the manufacturing industry has been difficult due to limitations in obtaining meaningful data from factories or mechanical systems. Accordingly, there have been active studies on manufacturing components with sensor integration allowing them to generate important data from themselves. Additive manufacturing enables the fabrication of a net shaped product with various materials including plastic, metal, or ceramic parts. With the principle of layer-bylayer adhesion of material, there has been active research to utilize this multi-step manufacturing process, such as changing the material at a certain step of adhesion or adding sensor components in the middle of the additive manufacturing process. Particularly for smart parts manufacturing, researchers have attempted to embed sensors or integrated circuit boards within a three-dimensional component during the additive manufacturing process. While most of the sensor embedding additive manufacturing was based on polymer material, there have also been studies on sensor integration within metal or ceramic materials. This study reviews the additive manufacturing technology for sensor integration into plastic, ceramic, and metal materials.

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Microstructures of Powders and Additively Manufactured Objects of an Alloy Tool Steel for Cold-Work Dies
Jun-Yun Kang, Jaecheol Yun, Hoyoung Kim, Byunghwan Kim, Jungho Choe, Sangsun Yang, Ji-Hun Yu, Yong-Jin Kim
J Korean Powder Metall Inst. 2016;24(3):202-209.   Published online June 1, 2016
DOI: https://doi.org/10.4150/KPMI.2017.24.3.202
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  • 3 Citations
AbstractAbstract PDF

A cold-work tool steel powder is used to fabricate 3-dimensional objects by selective laser melting using a high-pressure gas atomization process. The spherical powder particles form continuous carbide networks among the austenite matrix and its decomposition products. The carbides comprise Nb-rich MC and Mo-rich M2C. In the SLM process, the process parameters such as the laser power (90 W), layer thickness (25 μm), and hatch spacing (80 μm) are kept fixed, while the scan speed is changed from 50 mm/s to 4000 mm/s. At a low scan speed of 50 mm/s, spherical cavities develop due to over melting, while they are substantially reduced on increasing the speed to 2000 mm/s. The carbide network spacing decreases with increasing speed. At an excessively high speed of 4000 mm/s, long and irregularly shaped cavities are developed due to incomplete melting. The influence of the scan pattern is examined, for which 1 × 1 mm2 blocks constituting a processing layer are irradiated in a random sequence. This island-type pattern exhibits the same effect as that of a low scan speed. Post processing of an object using hot isostatic pressing leads to a great reduction in the porosity but causes coarsening of the microstructure.

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Citations to this article as recorded by  
  • Nanoindentation Creep Behavior of Additively Manufactured H13 Steel by Utilizing Selective Laser Melting Technology
    Evangelos Giarmas, Emmanouil K. Tzimtzimis, Nikolaos Kladovasilakis, Dimitrios Tzovaras, Dimitrios Tzetzis
    Materials.2024; 17(15): 3756.     CrossRef
  • Micro-Texture Analyses of a Cold-Work Tool Steel for Additive Manufacturing
    Jun-Yun Kang, Jaecheol Yun, Byunghwan Kim, Jungho Choe, Sangsun Yang, Seong-Jun Park, Ji-Hun Yu, Yong-Jin Kim
    Materials.2020; 13(3): 788.     CrossRef
  • Microstructural effects on the tensile and fracture behavior of selective laser melted H13 tool steel under varying conditions
    Jungsub Lee, Jungho Choe, Junhyeok Park, Ji-Hun Yu, Sangshik Kim, Im Doo Jung, Hyokyung Sung
    Materials Characterization.2019; 155: 109817.     CrossRef
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Mechanical Property Improvement of the H13 Tool Steel Sculptures Built by Metal 3D Printing Process via Optimum Conditions
Jaecheol Yun, Jungho Choe, Haengna Lee, Ki-Bong Kim, Sangsun Yang, Dong-Yeol Yang, Yong-Jin Kim, Chang-Woo Lee, Ji-Hun Yu
J Korean Powder Metall Inst. 2016;24(3):195-201.   Published online June 1, 2016
DOI: https://doi.org/10.4150/KPMI.2017.24.3.195
  • 237 View
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  • 7 Citations
AbstractAbstract PDF

In this study, H13 tool steel sculptures are built by a metal 3D printing process at various laser scan speeds. The properties of commercial H13 tool steel powders are confirmed for the metal 3D printing process used: powder bed fusion (PBF), which is a selective laser melting (SLM) process. Commercial H13 powder has an excellent flowability of 16.68 s/50 g with a Hausner ratio of 1.25 and a density of 7.68 g/cm3. The sculptures are built with dimensions of 10 × 10 × 10 mm3 in size using commercial H13 tool steel powder. The density measured by the Archimedes method is 7.64 g/cm3, similar to the powder density of 7.68 g/cm3. The hardness is measured by Rockwell hardness equipment 5 times to obtain a mean value of 54.28 HRC. The optimum process conditions in order to build the sculptures are a laser power of 90 W, a layer thickness of 25 μm, an overlap of 30%, and a laser scan speed of 200 mm/s.

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  • Spheroidization of Enamel Powders by Radio Frequency Plasma Treatment and Application to Additive Manufacturing
    Ki-Bong Kim, Dong-Yeol Yang, Yong-Jin Kim, Jungho Choe, Ji-Na Kwak, Woo-Hyung Jung
    Journal of Korean Powder Metallurgy Institute.2020; 27(5): 388.     CrossRef
  • Microstructural effects on the tensile and fracture behavior of selective laser melted H13 tool steel under varying conditions
    Jungsub Lee, Jungho Choe, Junhyeok Park, Ji-Hun Yu, Sangshik Kim, Im Doo Jung, Hyokyung Sung
    Materials Characterization.2019; 155: 109817.     CrossRef
  • Nano-mechanical Behavior of H13 Tool Steel Fabricated by a Selective Laser Melting Method
    Van Luong Nguyen, Eun-ah Kim, Jaecheol Yun, Jungho Choe, Dong-yeol Yang, Hak-sung Lee, Chang-woo Lee, Ji-Hun Yu
    Metallurgical and Materials Transactions A.2019; 50(2): 523.     CrossRef
  • Correlation between Microstructure and Mechanical Properties of the Additive Manufactured H13 Tool Steel
    Woojin An, Junhyeok Park, Jungsub Lee, Jungho Choe, Im Doo Jung, Ji-Hun Yu, Sangshik Kim, Hyokyung Sung
    Korean Journal of Materials Research.2018; 28(11): 663.     CrossRef
  • Evaluation of Strain-Rate Sensitivity of Selective Laser Melted H13 Tool Steel Using Nanoindentation Tests
    Van Luong Nguyen, Eun-ah Kim, Seok-Rok Lee, Jaecheol Yun, Jungho Choe, Dong-yeol Yang, Hak-sung Lee, Chang-woo Lee, Ji-Hun Yu
    Metals.2018; 8(8): 589.     CrossRef
  • Comparison of Nano-Mechanical Behavior between Selective Laser Melted SKD61 and H13 Tool Steels
    Jaecheol Yun, Van Luong Nguyen, Jungho Choe, Dong-Yeol Yang, Hak-Sung Lee, Sangsun Yang, Ji-Hun Yu
    Metals.2018; 8(12): 1032.     CrossRef
  • A study about sculpture characteristic of SKD61 tool steel fabricated by selective laser melting(SLM) process
    Jaecheol Yun, Jungho Choe, Ki-Bong Kim, Sangsun Yang, Dong-Yeol Yang, Yong-Jin Kim, Chang-Woo Lee, Chang-Woo Lee
    Journal of Korean Powder Metallurgy Institute.2018; 25(2): 137.     CrossRef
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The Influence of a Single Melt Pool Morphology on Densification Behavior of Three-Dimensional Structure Fabricated by Additive Manufacturing
Jungho Choe, Jaecheol Yun, Dong-Yeol Yang, Sangsun Yang, Ji-Hun Yu, Chang-Woo Lee, Yong-Jin Kim
J Korean Powder Metall Inst. 2016;24(3):187-194.   Published online June 1, 2016
DOI: https://doi.org/10.4150/KPMI.2017.24.3.187
  • 119 View
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  • 5 Citations
AbstractAbstract PDF

Selective laser melting (SLM) can produce a layer of a metal powder and then fabricate a three-dimensional structure by a layer-by-layer method. Each layer consists of several lines of molten metal. Laser parameters and thermal properties of the materials affect the geometric characteristics of the melt pool such as its height, depth, and width. The geometrical characteristics of the melt pool are determined herein by optical microscopy and three-dimensional bulk structures are fabricated to investigate the relationship between them. Powders of the commercially available Fe-based tool steel AISI H13 and Ni-based superalloy Inconel 738LC are used to investigate the effect of material properties. Only the scan speed is controlled to change the laser parameters. The laser power and hatch space are maintained throughout the study. Laser of a higher energy density is seen to melt a wider and deeper range of powder and substrate; however, it does not correspond with the most highly densified three-dimensional structure. H13 shows the highest density at a laser scan speed of 200 mm/s whereas Inconel 738LC shows the highest density at 600 mm/s.

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  • Microstructural effects on the tensile and fracture behavior of selective laser melted H13 tool steel under varying conditions
    Jungsub Lee, Jungho Choe, Junhyeok Park, Ji-Hun Yu, Sangshik Kim, Im Doo Jung, Hyokyung Sung
    Materials Characterization.2019; 155: 109817.     CrossRef
  • Correlation between Microstructure and Mechanical Properties of the Additive Manufactured H13 Tool Steel
    Woojin An, Junhyeok Park, Jungsub Lee, Jungho Choe, Im Doo Jung, Ji-Hun Yu, Sangshik Kim, Hyokyung Sung
    Korean Journal of Materials Research.2018; 28(11): 663.     CrossRef
  • Effect of Porosity on Mechanical Anisotropy of 316L Austenitic Stainless Steel Additively Manufactured by Selective Laser Melting
    Jeong Min Park, Jin Myoung Jeon, Jung Gi Kim, Yujin Seong, Sun Hong Park, Hyoung Seop Kim
    Journal of Korean Powder Metallurgy Institute.2018; 25(6): 475.     CrossRef
  • Evaluation of the Accuracy of Dental Prostheses manufactured by Metal 3D Printer
    Junho Hwang, Yun-Ho Kim, Hyun-Deok Kim, Kyu-Bok Lee
    Journal of Welding and Joining.2018; 36(5): 70.     CrossRef
  • A study about sculpture characteristic of SKD61 tool steel fabricated by selective laser melting(SLM) process
    Jaecheol Yun, Jungho Choe, Ki-Bong Kim, Sangsun Yang, Dong-Yeol Yang, Yong-Jin Kim, Chang-Woo Lee, Chang-Woo Lee
    Journal of Korean Powder Metallurgy Institute.2018; 25(2): 137.     CrossRef
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Trend in Research and Development Related to Lean Heavy Rare-earth Permanent Magnets for Next-generation Motors
Jung-Goo Lee, Youn-Kyoung Baek, Ji-Hun Yu, Chul-Jin Choi
J Korean Powder Metall Inst. 2012;19(2):151-159.
DOI: https://doi.org/10.4150/KPMI.2012.19.2.151
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  • 3 Citations
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  • Study on the Demagnetization and Classification of NdFeB Magnets According to Different Heat Treatment Temperatures
    Byeong Jun Kim, Ik Keun Park, Young Sung Kim
    Journal of the Korean Society of Manufacturing Technology Engineers.2021; 30(2): 119.     CrossRef
  • Low Cost Design Study of Brushless DC Motor for Electric Water Pump Application
    Tae-Uk Jung
    Journal of Electrical Engineering and Technology.2014; 9(3): 942.     CrossRef
  • Optimized Design of Rotor Considering Cost-Reduction of Small BLDC Motor for the Water Pump
    Hoe-Cheon Kim, Tae-Uk Jung
    The Transactions of The Korean Institute of Electrical Engineers.2013; 62(4): 495.     CrossRef
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Synthesis of Zr-Ti Alloy Powder by Magnesium Reduction
Dong-Won Lee, Geun-Tae Park, Tae-Soo Lim, Hye-Moon Lee, Ji-Hun Yu
J Korean Powder Metall Inst. 2011;18(4):359-364.
DOI: https://doi.org/10.4150/KPMI.2011.18.4.359
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AbstractAbstract PDF
Zr-Ti alloy powders were successfully synthesized by magnesium thermal reduction of metal chlorides. The evaporated and mixed gasses of ZrCl_4+TiCl_4 were injected to liquid magnesium and the chloride components were reduced by magnesium leading to the formation of MgCl_2. The released Zr and Ti atoms were then condensed to particle forms inside the mixture of liquid magnesium and magnesium chloride, which could be dissolved fully in post process by 1~5% HCl solution at room temperature. By the fraction-control of individually injected ZrCl_4 and TiCl_4 gasses, the final compositions of produced alloy powders were changed in the ranges of Zr-0 wt.%~20 wt.%Ti and their purity and particle size were about 99.4% and the level of several micrometers, respectively.

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  • Synthesis of Vanadium Powder by Magnesiothermic Reduction
    Dong Won Lee, Hak Sung Lee, Jung Yeul Yun, Young Ho Kim, Jei Pil Wang
    Advanced Materials Research.2014; 1025-1026: 509.     CrossRef
  • Extraction of Vanadium Powder by Metallothermic Reduction
    Dong-Won Lee, Sang-Hyun Heo, Jong-Taek Yeom, Jei-Pil Wang
    Journal of Korean Powder Metallurgy Institute.2013; 20(1): 43.     CrossRef
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A study on Magnetic Properties of BaFe12O19 Fabricated by Ultrasonic Spray-pyrolysis Process Using Self-Assembly Method
Moon-Hee Choi, Ji-Hun Yu, Dong-Hwan Kim, Kook-Chae Chung, Yang-Do Kim
J Korean Powder Metall Inst. 2010;17(4):263-269.
DOI: https://doi.org/10.4150/KPMI.2010.17.4.263
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AbstractAbstract PDF
Hexagonal barium ferrite (BaFe_12O_19) nano-particles have been successfully fabricated by spraypylorysis process. BaFe_12O_19 precursor solutions were synthesized by self-assembly method. Diethyleneamine (DEA) surfactant was used to fabricate the micelle structure of Ba-DEA complex under various DEA concentrations. BaFe_12O_19 powders were synthesized with addition of Fe ions to Ba-DEA complex and then fabricated BaFe_12O_19 powders by spray-pyrolysis process at the temperature range of 800sim1000°C. The molar ratio of Ba/DEA and heat-treatment temperatures significantly affected the magnetic properties and morphology of BaFe_12O_19 powders. BaFe_12O_19 powders synthesized with Ba/DEA molar ratio of 1 and heat-treated at 900°C showed the coercive forces (iHc) of 4.2 kOe with average crystal size of about 100 nm.

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  • Synthesize of Nd2Fe14B Powders from 1-D Nd2Fe14B Wires using Electrospinning Process
    Nu Si A Eom, Su Noh, Muhammad Aneeq Haq, Bum Sung Kim
    Journal of Korean Powder Metallurgy Institute.2019; 26(6): 477.     CrossRef
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The Present Issues of Rare Earth Magnetic Powder for Bonded Magnets
Dong-Hwan Kim, Ji-Hun Yu
J Korean Powder Metall Inst. 2010;17(2):81-87.
DOI: https://doi.org/10.4150/KPMI.2010.17.2.081
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  • 1 Citations
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  • Preparation of Highly Efficient Nd-Fe-B Magnetic Powders by Reduction/Diffusion Process
    Dongsoo Kim, Chunqiang Chen, Younkyoung Baek, Chuljin Choi
    Journal of Korean Powder Metallurgy Institute.2013; 20(3): 197.     CrossRef
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A Study on Magnetic Properties of BaFe12O_19 Fabricated by Self-assembly Method
Moon-Hee Choi, Ji-Hun Yu, Dong-Hwan Kim, Hye-Mum Lee, Su-Min Kim, Yang-Do Kim
J Korean Powder Metall Inst. 2009;16(6):410-415.
DOI: https://doi.org/10.4150/KPMI.2009.16.6.410
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AbstractAbstract PDF
Hexagonal barium ferrite (BaFe_12O_19) nano-particles have been successfully synthesised using selfassembly method. Diethyleneamine (DEA) surfactant was used to fabricate the micelle structure of Ba-DEA complex under various DEA concentrations. BaFe_12O_19 powders were synthesized with addition Fe ions to Ba-DEA complex and then heat treated at temperature range of 800-1000°C. The molar ratio of Ba/DEA and heat-treatment temperature significantly affected the magnetic properties and morphology of BaFe_12O_19 powders. BaFe_12O_19 powders synthesized with Ba/DEA molar ratio of 1 and heat-treated at 1000°C for 1 hour showed the coercive forces (iHc) of 4.84 kOe with average crystal size of about 200 nm.

Citations

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  • A study on Magnetic Properties of BaFe12O19Fabricated by Ultrasonic Spray-pyrolysis Process Using Self-Assembly Method
    Moon-Hee Choi, Ji-Hun Yu, Dong-Hwan Kim, Kook-Chae Chung, Yang-Do Kim
    Journal of Korean Powder Metallurgy Institute.2010; 17(4): 263.     CrossRef
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Characteristics of L10 Ordered Fe50Pt50 Nanoparticles Synthesized by Chemical Vapor Condensation Process
Gyeong-Mo Lee, Ji-Hun Yu, Dong-Won Lee, Byung-Kee Kim, Hyeok-Don Kim, Tae-Suk Jang
J Korean Powder Metall Inst. 2007;14(5):281-286.
DOI: https://doi.org/10.4150/KPMI.2007.14.5.281
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AbstractAbstract PDF
Ordered L1_0 to FePt nanoparticles are strong candidates for high density magnetic data storage media because the L1_0 phase FePt has a very high magnetocrystalline anisotropy (K_usim6.6-10times107erg/cm3), high coercivity and chemical stability. In this study, the ordered L1_0 FePt nanoparticles were successfully fabricated by chemical vapor condensation process without a post-annealing process which causes severe particle growth and agglomeration. The Fe_50Pt_50 nanopowder was obtained when the mixing ratio of Fe(acac) and Pt(arac) was 2.5 : 1. And the synthesized FePt nanoparticles were very fine and spherical shape with a narrow size distribution. The average particle size of the powder tended to increase from 5 nm to 10 nm with increasing reaction temperature from 800°C to 1000°C. Characterisitcs of FePt nanopowder were investigated in terms of process parameters and microstructures.

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